Short Description Rapid Computer Controlled Determinator CESA 40 TOC
With this Computer Controlled Elementary Determinator CESA 40 TOC
with up to 20-times automatic Sample transfer you can get quick and
reliable determinations of TOC / DOC, TIC and TC in organic and inorganic
materials like pure water, drinking water, surface water, ocean water,
sewage, swimming pool water, chemical industries water, purification
plants water, breweries water, in sewage sludge, sediments, waste,
compost, and seil.
Easy Operation allows you to operate this computer by semi-skilled
workpersons.
With the help of your Computer Controlled Determinator
you can get quick and reliable determination.
Industrial production processes are becoming more and more automated.
The features of this modern Determinator are an IBM-compatible Computer
with color-monitor and printer, electronic balance, and maintenance
physics (Infrared-measuringesystem) with up to 20-time automatic Sample
transfer.
Operation and Analysis of TOC / DOC, TIC and TC
TOC is the sum of organic bound carbon in solved and
unsolved organic compounds. DOC is the sum of
carbon contained in solved organic compounds. (0.45 ~m filtered).
Insert your TOC-samples #1 up to #20 in a ceramic boat
and place them on the balance. The computer keeps
the weight and other parameters in memory. Insert the ceramic boat
into the sample carousel. You also can use glazed ceramic boats. All
samples are combusted individual at temperatures of 600 - 1000 °C
in a quartztube. After the water is steamed suddenly and the contained
carbon is burned, the combustion-gases are fed to a peltiercooler,
a catalyst, to absorption traps and to the infrared measuring system-
The infrared measuring system sends an electric signal to the Computer.
The peak area integral of the C02-signal is direct proportional to
the TOC-value. The contained carbon from carbonide, bicarbonide or
solved carbondioxide in the water samples are seized by the Oxidation
with TOC and the sum is TC. With gas venting'of TIC in an acid milieu
you can determine the TOC value by substracting TC minus TIC. This
is only valid, if the TOC- and the TIC- concentration is nearly of
the saure value.
The determination of TTC is the saure with the adding
of phosphoric acid at a temperature of ca. 200 °C in
the quartztube. The set free carbonides are also measured by the infrared
system. Is the TIC-value higher
than the TOC-value, you have to dissolve TIC by aciding and gas venting.
Then you can determine TOC
directly.
To determine DOC , you have to remove anorganic bound
carbon from the sample by aciding and stripping. Operation and analysis
is as before.
At the end of every cycle the pneumatic-cylinder will
throw out the ceramic boat. All importantes parameters
like combustion-gasflow, combustions-curve, results, time, the name
of the Operator etc., will show up on the color monitor and will also
be saved to the hard-disc. There is a graphic printer connected to
the system for printing the results.
The system is measuring continuosly during every cycle.
One cycle from start of analysis to the end is approx. 90 seconds.
The maintenance of the traps, combustion-tube
and the filters need little Service
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